(2019) Application of selective solid-phase extraction using a new core-shell-shell magnetic ion-imprinted polymer for the analysis of ultra-trace mercury in serum of gallstone patients. Separation Science and Technology. p. 14. ISSN 0149-6395
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Abstract
A new ultrasonically assisted spectrophotometric method was developed using stabilized ion polymer on a modified nano-absorbent as a core- shell-shell absorbent (Fe3O4@SiO2@TiO2-IIP). It has the advantages of further stabilizing the polymer and consequently and much higher efficiency than its conventional adsorbents. The prepared sorbent was characterized and Its parameters were investigated by a Box-Behnken design. The linear dynamic range and limit of detection were 0.20-28.00 mu g L-1 and 0.05 mu g L-1 respectively. In selectivity study, it was founded that imprinting causes increased affinity of the prepared IIP toward Hg2+ ion. The proposed IIP is considered to be promising and selective sorbent for solid-phase extraction and preconcentration of Hg2+ ion in sera of different types of gallstone patients.
| Item Type: | Article | ||||||||
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| Keywords: | Magnetic ion imprinted polymer mercury preconcentration & xfeff Box-& xfeff Behnken design gallstone patients glassy-carbon electrode voltammetric sensor nanomolar detection paste electrode nanoparticles preconcentration adsorption gallbladder recommendations speciation Chemistry Engineering | ||||||||
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| Page Range: | p. 14 | ||||||||
| Journal or Publication Title: | Separation Science and Technology | ||||||||
| Journal Index: | ISI | ||||||||
| Identification Number: | https://doi.org/10.1080/01496395.2019.1651337 | ||||||||
| ISSN: | 0149-6395 | ||||||||
| Depositing User: | مهندس مهدی شریفی | ||||||||
| URI: | http://eprints.medilam.ac.ir/id/eprint/2358 |
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